2W26

Factor Xa in complex with BAY59-7939

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS
Synchrotron site	SLS
Temperature [K]	100
Spacegroup name	P 21 21 21
Unit cell lengths	56.042, 72.028, 78.446
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	20.000 - 2.080
R-factor	0.2198
Rwork	0.220
R-free	0.25910
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.011
RMSD bond angle	1.558
Data reduction software	XDS
Data scaling software	XDS
Refinement software	CNS

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	20.000	2.170
High resolution limit [Å]	2.080	2.080
Rmerge	0.080
Number of reflections	18961
<I/σ(I)>	12.6	3.2
Completeness [%]	94.3	71.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1