2W0K
Crystal structure of the recombinant variable domain 6JAL2
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | NSLS BEAMLINE X6A |
| Synchrotron site | NSLS |
| Beamline | X6A |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2005-05-24 |
| Detector | ADSC CCD |
| Spacegroup name | P 41 2 2 |
| Unit cell lengths | 71.267, 71.267, 95.452 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 22.630 - 2.350 |
| R-factor | 0.212 |
| Rwork | 0.209 |
| R-free | 0.24200 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2cd0 |
| RMSD bond length | 0.032 |
| RMSD bond angle | 3.124 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.190 | 2.480 |
| High resolution limit [Å] | 2.350 | 2.350 |
| Rmerge | 0.050 | 0.390 |
| Number of reflections | 9289 | |
| <I/σ(I)> | 15.5 | 2.8 |
| Completeness [%] | 87.9 | 92.4 |
| Redundancy | 3 | 2.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
