2VZS
Chitosan Product complex of Amycolatopsis orientalis exo-chitosanase CsxA
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU MICROMAX-002 |
| Temperature [K] | 113 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 86.544, 121.810, 91.843 |
| Unit cell angles | 90.00, 90.42, 90.00 |
Refinement procedure
| Resolution | 40.000 - 1.850 |
| R-factor | 0.175 |
| Rwork | 0.173 |
| R-free | 0.22000 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.018 |
| RMSD bond angle | 1.746 |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 20.000 |
| High resolution limit [Å] | 1.850 |
| Rmerge | 0.090 |
| Number of reflections | 153524 |
| <I/σ(I)> | 8.1 |
| Completeness [%] | 99.9 |
| Redundancy | 4.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
