2VZR

C-terminal CBM35 from Amycolatopsis orientalis exo-chitosanase CsxA in complex with glucuronic acid

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU MICROMAX-002
Temperature [K]	113
Spacegroup name	P 21 21 21
Unit cell lengths	54.569, 56.981, 81.352
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	20.000 - 1.950
R-factor	0.186
Rwork	0.183
R-free	0.24800
Structure solution method	OTHER
RMSD bond length	0.011
RMSD bond angle	1.265
Refinement software	REFMAC (5.2.0019)

Data quality characteristics

	Overall
Low resolution limit [Å]	19.710
High resolution limit [Å]	1.950
Rmerge	0.090
Number of reflections	18625
<I/σ(I)>	8.9
Completeness [%]	97.7
Redundancy	4.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1