2VZQ

C-terminal CBM35 from Amycolatopsis orientalis exo-chitosanase CsxA in complex with digalacturonic acid

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU MICROMAX-002
Temperature [K]	113
Spacegroup name	P 1 21 1
Unit cell lengths	28.925, 54.772, 81.341
Unit cell angles	90.00, 100.16, 90.00

Refinement procedure

Resolution	80.060 - 1.700
R-factor	0.174
Rwork	0.171
R-free	0.21700
Structure solution method	OTHER
RMSD bond length	0.019
RMSD bond angle	1.736
Refinement software	REFMAC (5.2.0019)

Data quality characteristics

	Overall
Low resolution limit [Å]	20.000
High resolution limit [Å]	1.700
Rmerge	0.100
Number of reflections	27317
<I/σ(I)>	9.2
Completeness [%]	98.8
Redundancy	6.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1