2VXK

Structural comparison between Aspergillus fumigatus and human GNA1

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE BM14
Synchrotron site	ESRF
Beamline	BM14
Temperature [K]	10
Detector technology	CCD
Detector	MARRESEARCH
Spacegroup name	C 2 2 21
Unit cell lengths	70.606, 100.826, 55.350
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	20.000 - 1.800
R-factor	0.179
Rwork	0.178
R-free	0.21800
Structure solution method	SAD
Starting model (for MR)	NONE
RMSD bond length	0.016
RMSD bond angle	1.546
Refinement software	REFMAC (5.2.0005)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	20.000	1.860
High resolution limit [Å]	1.800	1.800
Rmerge	0.030	0.150
Number of reflections	18376
<I/σ(I)>	21.2	10.5
Completeness [%]	98.2	98
Redundancy	4.6	4.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1