2VXG
Crystal structure of the conserved C-terminal region of Ge-1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-09-15 |
Detector | MARRESEARCH |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 38.240, 65.870, 103.780 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 55.640 - 1.900 |
R-factor | 0.213 |
Rwork | 0.211 |
R-free | 0.25400 |
Structure solution method | SAD |
Starting model (for MR) | NONE |
RMSD bond length | 0.017 |
RMSD bond angle | 1.477 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | SHARP |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 55.600 | 2.000 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.070 | 0.440 |
Number of reflections | 20948 | |
<I/σ(I)> | 15.9 | 2.5 |
Completeness [%] | 98.0 | 88.8 |
Redundancy | 4.1 | 3.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8.2 | 100 MM TRIS-CL PH 8.2 21% (W/V) PEG 3350 |