2VUR

Chemical dissection of the link between Streptozotocin, O-GlcNAc and pancreatic cell death

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID14-4
Synchrotron site	ESRF
Beamline	ID14-4
Temperature [K]	100
Detector technology	CCD
Collection date	2006-08-30
Detector	ADSC CCD
Spacegroup name	I 21 21 21
Unit cell lengths	130.470, 149.731, 152.121
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	19.910 - 2.200
R-factor	0.196
Rwork	0.195
R-free	0.24100
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.012
RMSD bond angle	1.309
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	MOLREP
Refinement software	REFMAC (5.2.0019)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	20.000	2.170
High resolution limit [Å]	2.100	2.100
Rmerge	0.060	0.370
Number of reflections	67062
<I/σ(I)>	22	2
Completeness [%]	99.8	99.3
Redundancy	3.6	3.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1