2VTW
Structure of the C-terminal head domain of the fowl adenovirus type 1 short fibre
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID14-4 |
| Synchrotron site | ESRF |
| Beamline | ID14-4 |
| Temperature [K] | 77 |
| Detector technology | CCD |
| Detector | ADSC CCD |
| Spacegroup name | P 41 21 2 |
| Unit cell lengths | 235.750, 235.750, 61.750 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 47.570 - 2.000 |
| R-factor | 0.177 |
| Rwork | 0.175 |
| R-free | 0.21400 |
| Structure solution method | SAD |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.015 |
| RMSD bond angle | 1.487 |
| Data reduction software | XDS |
| Phasing software | SHELXD |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 47.600 | 2.100 |
| High resolution limit [Å] | 2.000 | 2.000 |
| Rmerge | 0.010 | 0.050 |
| Number of reflections | 117179 | |
| <I/σ(I)> | 8.99 | 3.19 |
| Completeness [%] | 99.8 | 100 |
| Redundancy | 3.63 | 3.61 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 0.1 M LITHIUM SULPHATE, 0.1 M TRI-SODIUM CITRATE AT PH 5.6 AND 12% W/V POLYETHYLENE GLYCOL (PEG) 4000 |
