2VSG

A Structural Motif in the Variant Surface Glycoproteins of Trypanosoma Brucei

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Temperature [K]	277
Detector technology	AREA DETECTOR
Collection date	1986-08-05
Detector	XENTRONICS
Spacegroup name	P 21 21 21
Unit cell lengths	55.100, 98.800, 172.900
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	6.000 - 2.700
Rwork	0.203
Structure solution method	SIRAS
RMSD bond length	0.019
RMSD bond angle	3.470
Data reduction software	ROTAVATA
Data scaling software	CCP4 ((AGROVATA)
Refinement software	X-PLOR

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	10.000	2.830
High resolution limit [Å]	2.700	2.700
Rmerge	0.102 *	0.390 *
Total number of observations	107903 *
Number of reflections	24682
Completeness [%]	93.0
Redundancy	4.4	3.64

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *	6.5		pH 6.5