2VOK
Murine TRIM21
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID14-3 |
| Synchrotron site | ESRF |
| Beamline | ID14-3 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Detector | ADSC CCD |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 62.955, 44.889, 71.794 |
| Unit cell angles | 90.00, 109.89, 90.00 |
Refinement procedure
| Resolution | 67.570 - 1.300 |
| R-factor | 0.215 |
| Rwork | 0.214 |
| R-free | 0.23600 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.270 |
| Refinement software | REFMAC (5.3.0022) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 29.230 |
| High resolution limit [Å] | 1.300 |
| Rmerge | 0.060 |
| Number of reflections | 92548 |
| <I/σ(I)> | 13 |
| Completeness [%] | 99.7 |
| Redundancy | 3.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
