2VMI

The structure of seleno-methionine labelled CBM51 from Clostridium perfringens GH95

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Temperature [K]	113
Spacegroup name	P 65
Unit cell lengths	76.721, 76.721, 51.771
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	66.370 - 1.700
R-factor	0.151
Rwork	0.150
R-free	0.17800
Structure solution method	SAD
Starting model (for MR)	NONE
RMSD bond length	0.020
RMSD bond angle	1.602
Refinement software	REFMAC (5.2.0019)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	20.000	1.760
High resolution limit [Å]	1.700	1.700
Rmerge	0.140	0.330
Number of reflections	18188
<I/σ(I)>	15.5	6.5
Completeness [%]	99.9	98.6
Redundancy	19.8	10.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1