Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE BM14 |
| Synchrotron site | ESRF |
| Beamline | BM14 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2006-11-14 |
| Detector | MARRESEARCH |
| Spacegroup name | P 65 |
| Unit cell lengths | 67.490, 67.490, 33.170 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 10.000 - 2.050 |
| R-factor | 0.171 |
| Rwork | 0.168 |
| R-free | 0.23800 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2QK6 |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.444 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.000 | 2.100 |
| High resolution limit [Å] | 2.050 | 2.050 |
| Rmerge | 0.080 | 0.620 |
| Number of reflections | 5525 | |
| <I/σ(I)> | 14.8 | 2.8 |
| Completeness [%] | 99.7 | 100 |
| Redundancy | 5.5 | 5.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 2.3M AMMONIUM SULPHATE, 0.1M TRIS-HCL, PH 8.5, VAPOR DIFFUSION, HANGING DROP |
