2VH3
ranasmurfin
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE BM14 |
| Synchrotron site | ESRF |
| Beamline | BM14 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Detector | MARRESEARCH |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 40.990, 59.670, 44.900 |
| Unit cell angles | 90.00, 93.31, 90.00 |
Refinement procedure
| Resolution | 44.810 - 1.160 |
| R-factor | 0.216 |
| Rwork | 0.214 |
| R-free | 0.23600 |
| Structure solution method | SAD |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.293 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 44.000 | 1.220 |
| High resolution limit [Å] | 1.160 | 1.160 |
| Rmerge | 0.040 | 0.630 |
| Number of reflections | 65500 | |
| <I/σ(I)> | 12 | 1.8 |
| Completeness [%] | 93.0 | 70 |
| Redundancy | 3.8 | 80 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 6 | pH 6 |
