2VG0
Rv1086 citronellyl pyrophosphate complex
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID14-3 |
| Synchrotron site | ESRF |
| Beamline | ID14-3 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Detector | ADSC CCD |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 58.517, 73.541, 102.561 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 26.610 - 1.700 |
| R-factor | 0.176 |
| Rwork | 0.173 |
| R-free | 0.21500 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.245 |
| Data reduction software | SCALA |
| Data scaling software | MOSFLM |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 27.000 | 1.900 |
| High resolution limit [Å] | 1.700 | 1.800 |
| Rmerge | 0.010 | |
| Number of reflections | 46922 | |
| <I/σ(I)> | 25 | |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 7.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
