Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU MICROMAX-007 |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Detector | RIGAKU IMAGE PLATE |
| Spacegroup name | P 21 3 |
| Unit cell lengths | 137.055, 137.055, 137.055 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 39.560 - 2.100 |
| R-factor | 0.211 |
| Rwork | 0.208 |
| R-free | 0.25200 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.186 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 39.560 | |
| High resolution limit [Å] | 2.100 | 2.100 |
| Rmerge | 0.060 | 0.450 |
| Number of reflections | 49729 | |
| <I/σ(I)> | 17.1 | 3.1 |
| Completeness [%] | 99.4 | 95.7 |
| Redundancy | 5.3 | 4.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 6.5 | 0.1 M MES PH 6.5, 0.2 M NACL AND 1.5 M (NH4)2SO4 |
