2V7L

PrnB 7Cl-L-tryptophan complex

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU MICROMAX-007
Temperature [K]	100
Detector technology	IMAGE PLATE
Detector	RIGAKU-MSC
Spacegroup name	C 1 2 1
Unit cell lengths	68.410, 78.883, 93.341
Unit cell angles	90.00, 104.11, 90.00

Refinement procedure

Resolution	90.540 - 2.400
R-factor	0.184
Rwork	0.182
R-free	0.21300
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	2v7j
RMSD bond length	0.009
RMSD bond angle	1.119
Data reduction software	MOSFLM
Data scaling software	SCALA (CCP4)
Refinement software	REFMAC (5.2.0019)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	39.000	2.500
High resolution limit [Å]	2.400	2.400
Rmerge	0.050	0.100
Number of reflections	17632
<I/σ(I)>	14	6
Completeness [%]	98.0	94.9
Redundancy	2.1	2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1		7.5		pH 7.5