2V78
Crystal structure of Sulfolobus solfataricus 2-keto-3-deoxygluconate kinase
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID14-1 |
| Synchrotron site | ESRF |
| Beamline | ID14-1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Detector | ADSC CCD |
| Spacegroup name | P 65 2 2 |
| Unit cell lengths | 104.865, 104.865, 422.502 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 46.980 - 2.000 |
| R-factor | 0.164 |
| Rwork | 0.162 |
| R-free | 0.19800 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.020 |
| RMSD bond angle | 1.799 |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 76.300 | 2.110 |
| High resolution limit [Å] | 2.000 | 2.000 |
| Rmerge | 0.060 | 0.210 |
| Number of reflections | 91205 | |
| <I/σ(I)> | 26.8 | 7.2 |
| Completeness [%] | 97.0 | 81.4 |
| Redundancy | 12.8 | 3.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
