2V10

Crystal Structure of Renin with Inhibitor 9

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	ENRAF-NONIUS FR571
Temperature [K]	100
Detector technology	AREA DETECTOR
Collection date	1991-01-01
Detector	DELFT INSTRUMENTS
Spacegroup name	P 21 3
Unit cell lengths	143.000, 143.000, 143.000
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	10.000 - 3.100
R-factor	0.21
Rwork	0.210
Structure solution method	OTHER
Data reduction software	MADNESS
Refinement software	TNT

Data quality characteristics

	Overall
Low resolution limit [Å]	10.000
High resolution limit [Å]	3.100
Rmerge	0.120
Number of reflections	17734
Completeness [%]	99.0
Redundancy	3.35

Crystallization Conditions

crystal ID	method	pH	temperature	details
1		4.5		pH 4.50