2UVP
Crystal structure of HobA (HP1230)from Helicobacter pylori
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-3 |
Synchrotron site | ESRF |
Beamline | ID14-3 |
Temperature [K] | 173 |
Detector technology | CCD |
Collection date | 2005-12-01 |
Detector | MARRESEARCH |
Spacegroup name | P 32 |
Unit cell lengths | 112.232, 112.232, 61.929 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 97.130 - 1.700 |
R-factor | 0.182 |
Rwork | 0.180 |
R-free | 0.21400 |
Structure solution method | SAD |
Starting model (for MR) | NONE |
RMSD bond length | 0.012 |
RMSD bond angle | 1.459 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | SHARP |
Refinement software | REFMAC (5.3.0011) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 41.590 | 1.790 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.060 | 0.310 |
Number of reflections | 95964 | |
<I/σ(I)> | 15.8 | 1.4 |
Completeness [%] | 100.0 | 99.9 |
Redundancy | 4.6 | 4.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5.5 | 100 MM MES PH 5.6, 300 MM CA ACETATE, 14-20% PEG 3350. | ||
1 | 5.5 | 100 MM MES PH 5.6, 300 MM CA ACETATE, 14-20% PEG 3350. |