2UVK
Structure of YjhT
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID14-4 |
| Synchrotron site | ESRF |
| Beamline | ID14-4 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2006-07-07 |
| Detector | ADSC CCD |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 44.758, 105.659, 74.222 |
| Unit cell angles | 90.00, 99.95, 90.00 |
Refinement procedure
| Resolution | 73.130 - 1.500 |
| R-factor | 0.182 |
| Rwork | 0.180 |
| R-free | 0.21900 |
| Structure solution method | SAD |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.306 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | SHELXCD |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 52.850 | 1.580 |
| High resolution limit [Å] | 1.500 | 1.500 |
| Rmerge | 0.040 | 0.380 |
| Number of reflections | 107873 | |
| <I/σ(I)> | 30.1 | 5.9 |
| Completeness [%] | 99.5 | 99.3 |
| Redundancy | 8.1 | 8.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7.5 | 150 NL OF SEMET-SUBSTITUTED YJHT AND 150 NL OF 200 MM SODIUM MALONATE, 0.1M BIS TRIS PROPANE PH 7.5 AND 20% W/V PEG 3350 |
