2UKD
UMP/CMP KINASE FROM SLIME MOLD COMPLEXED WITH ADP, CMP
Experimental procedure
Source type | SYNCHROTRON |
Source details | EMBL/DESY, HAMBURG BEAMLINE BW7B |
Synchrotron site | EMBL/DESY, HAMBURG |
Beamline | BW7B |
Temperature [K] | 277 |
Detector technology | IMAGE PLATE |
Collection date | 1996-08-01 |
Detector | MARRESEARCH |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 78.700, 78.700, 100.100 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 37.000 - 2.200 |
R-factor | 0.193 |
Rwork | 0.193 |
R-free | 0.23100 |
Structure solution method | DIFFERENCE FOURIER |
RMSD bond length | 0.011 |
RMSD bond angle | 1.190 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | X-PLOR (3.851) |
Refinement software | X-PLOR (3.851) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 37.000 | 2.320 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.074 | 0.221 |
Total number of observations | 53982 * | |
Number of reflections | 15558 | |
Completeness [%] | 94.0 | 95 |
Redundancy | 3.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 8.5 | pH 8.5 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | UmpKdicty | 0.64 (mM) | |
2 | 1 | 1 | ADP | 0.8 (mM) | |
3 | 1 | 1 | CMP | 0.8 (mM) | or UMP |
4 | 1 | 1 | Tris-HCl | 100 (mM) | |
5 | 1 | 1 | 30 (mM) | ||
6 | 1 | 1 | DTE | 40 (mM) | |
7 | 1 | 1 | 0.8 (mM) | or BeCl2 | |
8 | 1 | 1 | 4 (mM) | ||
9 | 1 | 2 | PEG4000 | precipitant |