2TRX

CRYSTAL STRUCTURE OF THIOREDOXIN FROM ESCHERICHIA COLI AT 1.68 ANGSTROMS RESOLUTION

Experimental procedure

Spacegroup name	C 1 2 1
Unit cell lengths	89.500, 51.060, 60.450
Unit cell angles	90.00, 113.50, 90.00

Refinement procedure

Resolution	8.000 - 1.680
R-factor	0.165
RMSD bond length	0.015
RMSD bond angle	0.035
Refinement software	PROFFT

Data quality characteristics

	Overall
Low resolution limit [Å]	2.500 *
High resolution limit [Å]	1.680 *
Number of reflections	27483 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Microdialysis *	3.8 *	4 *	equilibrium dialysis *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	MPD	40 (%(v/v))
2	1	reservior	sodium acetate	0.01 (M)
3	1	reservoir	cupric acetatae	1 (mM)