2TPI
ON THE DISORDERED ACTIVATION DOMAIN IN TRYPSINOGEN. CHEMICAL LABELLING AND LOW-TEMPERATURE CRYSTALLOGRAPHY
Experimental procedure
| Spacegroup name | I 2 2 2 |
| Unit cell lengths | 75.670, 84.160, 122.890 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 6.500 - 2.100 |
| R-factor | 0.2 * |
| Rwork | 0.200 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion * | 7 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | drop | protein | 10 (mg/ml) | |
| 2 | 1 | drop | pancreatic trypsin inhibitor | equimolar amount | |
| 3 | 1 | drop | Ile-Val dipeptide | 3.5 (mg/ml) | |
| 4 | 1 | drop | 1.5 (M) | ||
| 5 | 1 | reservoir | 1.5 (M) |
