Experimental procedure
| Source type | ROTATING ANODE |
| Source details | RIGAKU RUH2R |
| Temperature [K] | 295 |
| Detector technology | AREA DETECTOR |
| Collection date | 1990-11 |
| Detector | SIEMENS |
| Spacegroup name | P 61 2 2 |
| Unit cell lengths | 78.600, 78.600, 240.200 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 7.000 - 2.550 |
| R-factor | 0.185 |
| Rwork | 0.185 |
| RMSD bond length | 0.008 |
| RMSD bond angle | 24.700 * |
| Data reduction software | XENGEN |
| Data scaling software | XENGEN |
| Refinement software | X-PLOR |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.700 |
| High resolution limit [Å] | 2.550 | 2.550 |
| Rmerge | 0.156 * | 0.520 * |
| Total number of observations | 46338 * | |
| Number of reflections | 12591 | |
| <I/σ(I)> | 9.4 | 0.8 |
| Completeness [%] | 83.0 | 65 |
| Redundancy | 3.7 | 2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion * | 7.4 | pH 7.4 |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | drop | protein | 10 (mg/ml) | |
| 2 | 1 | reservoir | potassium phosphate | 20 (mM) | |
| 3 | 1 | reservoir | ammonium sulfate | 20 (mM) |
