2SOD

DETERMINATION AND ANALYSIS OF THE 2 ANGSTROM STRUCTURE OF COPPER, ZINC SUPEROXIDE DISMUTASE

Replaces:  1SOD

Experimental procedure

Spacegroup name	C 1 2 1
Unit cell lengths	93.650, 90.330, 71.650
Unit cell angles	90.00, 95.10, 90.00

Refinement procedure

Resolution	4.000 * - 2.000
R-factor	0.255 *
Rwork	0.256
RMSD bond length	0.030 *
Refinement software	PROLSQ

Data quality characteristics

	Overall
Low resolution limit [Å]	4.000 *
High resolution limit [Å]	2.000 *
Number of reflections	17206 *
Completeness [%]	35.0 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *	7.5 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	enzyme	1.5 (mg/ml)
2	1	reservoir	phosphate	0.5 (M)
3	1	reservoir	MPD	58 (%(v/v))