2SBL
THE THREE-DIMENSIONAL STRUCTURE OF AN ARACHIDONIC ACID 15-LIPOXYGENASE
Experimental procedure
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 184.500, 125.600, 94.700 |
| Unit cell angles | 90.00, 102.90, 90.00 |
Refinement procedure
| Resolution | ? - 2.600 |
| R-factor | 0.173 |
| Rwork | 0.173 |
| RMSD bond length | 0.010 |
| RMSD bond angle | 2.700 |
| Phasing software | X-PLOR (3.1) |
| Refinement software | X-PLOR (3.1) |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | reservoir | sodium formate | 4.6 (M) | |
| 2 | 1 | reservoir | ammonium acetate | 1.0 (M) | |
| 3 | 1 | reservoir | lithium chloride | 600 (mM) | |
| 4 | 1 | reservoir | 2-(N-morpholino)ethanesulfonic acid | 20 (mM) | |
| 5 | 1 | drop | protein | 15-20 (mg/ml) |
