2ROY

TRANSTHYRETIN (ALSO CALLED PREALBUMIN) COMPLEX WITH 3',5'-DINITRO-N-ACETYL-L-THYRONINE

Replaces:  1ROY

Experimental procedure

Spacegroup name	P 21 21 2
Unit cell lengths	43.621, 86.041, 64.953
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	8.000 - 2.200
R-factor	0.184 *
Rwork	0.184
RMSD bond length	0.020
RMSD bond angle	0.060
Refinement software	PROLSQ

Data quality characteristics

	Overall
High resolution limit [Å]	2.200 *
Rmerge	0.069 *
Total number of observations	70011 *
Number of reflections	12450 *
Completeness [%]	96.2 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *	6.9 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	phosphate	10 (mM)
2	1	reservoir	ammonium sulfate	55 (%)
3	1	reservoir	phosphate	0.1 (M)