2R91

Crystal Structure of KD(P)GA from T.tenax

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X10SA
Synchrotron site	SLS
Beamline	X10SA
Temperature [K]	100
Detector technology	CCD
Collection date	2005-04-20
Detector	MARMOSAIC 225 mm CCD
Wavelength(s)	0.905
Spacegroup name	P 43 21 2
Unit cell lengths	150.347, 150.347, 175.420
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	48.170 - 2.000
R-factor	0.186
Rwork	0.184
R-free	0.21300
RMSD bond length	0.016
RMSD bond angle	1.472
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	PHASER
Refinement software	REFMAC (5.2.0019)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	48.170	2.100
High resolution limit [Å]	2.000	2.000
Rmerge	0.065	0.250
Number of reflections	135046
<I/σ(I)>		5.92
Completeness [%]		100
Redundancy	9.9	10

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION	7	298	HEPES/KOH, pH 7.0, VAPOR DIFFUSION, temperature 298K