2R8X

Crystal structure of YrbI phosphatase from Escherichia coli

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 21-ID-D
Synchrotron site	APS
Beamline	21-ID-D
Detector technology	CCD
Collection date	2007-04-13
Detector	MARMOSAIC 225 mm CCD
Spacegroup name	P 1 21 1
Unit cell lengths	85.071, 156.959, 114.407
Unit cell angles	90.00, 96.54, 90.00

Refinement procedure

Resolution	30.000 - 2.600
R-factor	0.20291
Rwork	0.201
R-free	0.23640
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.006
RMSD bond angle	0.864
Refinement software	REFMAC (5.2.0019)

Data quality characteristics

	Overall
Low resolution limit [Å]	39.800
High resolution limit [Å]	2.600
Number of reflections	86138

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP			VAPOR DIFFUSION, HANGING DROP