2R60
Structure of apo Sucrose Phosphate Synthase (SPS) of Halothermothrix orenii
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | NSLS BEAMLINE X12C |
| Synchrotron site | NSLS |
| Beamline | X12C |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2006-04-05 |
| Detector | ADSC QUANTUM 210 |
| Wavelength(s) | 0.9788 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 154.225, 48.499, 75.051 |
| Unit cell angles | 90.00, 100.92, 90.00 |
Refinement procedure
| Resolution | 20.000 - 1.800 |
| Rwork | 0.226 |
| R-free | 0.25200 |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.404 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | SOLVE |
| Refinement software | CNS |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 1.860 |
| High resolution limit [Å] | 1.800 | 1.800 |
| Number of reflections | 49698 | |
| <I/σ(I)> | 12.1 | |
| Completeness [%] | 97.2 | 75.9 |
| Redundancy | 6.7 | 4.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
