2R5I

Pentamer Structure of Major Capsid Protein L1 of Human Papilloma Virus type 18

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALS BEAMLINE 4.2.2
Synchrotron site	ALS
Beamline	4.2.2
Temperature [K]	100
Detector technology	CCD
Spacegroup name	P 1
Unit cell lengths	81.161, 105.039, 235.749
Unit cell angles	87.56, 85.66, 68.16

Refinement procedure

Resolution	40.000 - 3.400
R-factor	0.21619
Rwork	0.214
R-free	0.26016
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.041
RMSD bond angle	2.761
Refinement software	REFMAC (5.2.0019)

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	3.400
Number of reflections	98881
<I/σ(I)>	4.4
Redundancy	3.55

Crystallization Conditions

crystal ID	method	pH	temperature	details
1