2R3Z

Crystal structure of mouse IP-10

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SRS BEAMLINE PX14.2
Synchrotron site	SRS
Beamline	PX14.2
Temperature [K]	100
Detector technology	CCD
Collection date	2004-09-07
Detector	ADSC QUANTUM 4
Wavelength(s)	0.98
Spacegroup name	C 1 2 1
Unit cell lengths	109.957, 71.530, 39.577
Unit cell angles	90.00, 111.08, 90.00

Refinement procedure

Resolution	19.790 - 2.500
R-factor	0.2754
Rwork	0.275
R-free	0.30820
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1o7y
RMSD bond length	0.010
RMSD bond angle	1.400
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	PHASER
Refinement software	CNS (1.1)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	2.570
High resolution limit [Å]	2.500	2.500
Rmerge	0.091	0.304
Number of reflections	9824
<I/σ(I)>		3.26
Completeness [%]	98.2	89.7
Redundancy	2.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	8	290	0.1M Tris-HCl, 0.2M CaCl2, 35% PEG3350, pH 8.0, VAPOR DIFFUSION, HANGING DROP, temperature 290K
1	VAPOR DIFFUSION, HANGING DROP	8	290	0.1M Tris-HCl, 0.2M CaCl2, 35% PEG3350, pH 8.0, VAPOR DIFFUSION, HANGING DROP, temperature 290K