2QZQ
Crystal structure of C-terminal of Aida
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PHOTON FACTORY BEAMLINE BL-6A |
| Synchrotron site | Photon Factory |
| Beamline | BL-6A |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2005-12-09 |
| Detector | ADSC QUANTUM 315 |
| Wavelength(s) | 0.9786 |
| Spacegroup name | P 32 2 1 |
| Unit cell lengths | 54.951, 54.951, 130.020 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 26.840 - 1.900 |
| R-factor | 0.197 |
| Rwork | 0.193 |
| R-free | 0.23000 |
| RMSD bond length | 0.016 |
| RMSD bond angle | 1.525 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | SOLVE |
| Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 47.560 | 2.000 |
| High resolution limit [Å] | 1.900 | 1.900 |
| Rmerge | 0.067 | 0.406 |
| Number of reflections | 18670 | |
| <I/σ(I)> | 33.9 | 9 |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 20.8 | 20.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 7.4 | 291 | 0.1 HEPES Na pH 7.4, 12% PEG 3350, 2% MPD, VAPOR DIFFUSION, temperature 291K |
