2QW7
Carboxysome Subunit, CcmL
Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | ALS BEAMLINE 8.2.2 |
| Synchrotron site | ALS |
| Beamline | 8.2.2 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2006-09-14 |
| Detector | ADSC QUANTUM 315 |
| Wavelength(s) | 0.97944, 0.979617, 0.975593 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 64.428, 107.444, 72.264 |
| Unit cell angles | 90.00, 96.51, 90.00 |
Refinement procedure
| Resolution | 19.900 - 2.400 |
| R-factor | 0.243 |
| Rwork | 0.240 |
| R-free | 0.29600 |
| Structure solution method | MAD |
| RMSD bond length | 0.018 |
| RMSD bond angle | 2.404 |
| Refinement software | REFMAC |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 90.000 |
| High resolution limit [Å] | 2.400 |
| Rmerge | 0.129 |
| Number of reflections | 52537 |
| <I/σ(I)> | 6.4 |
| Completeness [%] | 98.0 |
| Redundancy | 3.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 298 | 0.1M bis-Tris, 20% PEG3350, 0.3M NaCl, pH 6.5, vapor diffusion, hanging drop, temperature 298K |
