2QDK

X-ray structure of the unliganded uridine phosphorylase from Salmonella typhimurium at 1.62A resolution

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	EMBL/DESY, HAMBURG BEAMLINE X11
Synchrotron site	EMBL/DESY, HAMBURG
Beamline	X11
Temperature [K]	100
Detector technology	CCD
Detector	MAR CCD 165 mm
Spacegroup name	P 21 21 21
Unit cell lengths	89.600, 125.030, 134.950
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	6.000 - 1.620
Rwork	0.191
Structure solution method	MOLECULAR REPLACEMENT
Refinement software	PHENIX

Data quality characteristics

	Overall
Low resolution limit [Å]	25.400
High resolution limit [Å]	1.600
Number of reflections	187456

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		297	VAPOR DIFFUSION, HANGING DROP, temperature 297K