2QB7
Saccharomyces cerevisiae cytosolic exopolyphosphatase, phosphate complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-1 |
Synchrotron site | ESRF |
Beamline | ID14-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.93400 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 79.992, 83.039, 118.900 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 67.420 - 1.600 |
R-factor | 0.17216 |
Rwork | 0.171 |
R-free | 0.20139 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2qb6 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.433 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | REFMAC (5.2.0005) |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 68.000 | 1.690 |
High resolution limit [Å] | 1.600 | 1.600 |
Number of reflections | 99085 | |
<I/σ(I)> | 5.8 | 2.8 |
Completeness [%] | 94.6 | 74.9 |
Redundancy | 3.7 | 2.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.6 | 291 | 7% PEG 4000, 150 mM (NH4)2SO4, pH 4.6, VAPOR DIFFUSION, HANGING DROP, temperature 291K |