2Q6I
salL with ClDA and LMet
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.2.2 |
Synchrotron site | ALS |
Beamline | 8.2.2 |
Detector technology | CCD |
Collection date | 2006-11-01 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1 |
Spacegroup name | P 63 2 2 |
Unit cell lengths | 111.030, 111.030, 93.310 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 19.940 - 2.600 |
R-factor | 0.20879 |
Rwork | 0.206 |
R-free | 0.26203 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1rqp |
RMSD bond length | 0.009 |
RMSD bond angle | 1.226 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.760 |
High resolution limit [Å] | 2.600 | 2.600 |
Number of reflections | 10922 | |
<I/σ(I)> | 19.39 | |
Redundancy | 14.92 | 14.65 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 277 | 28% PEG3350, 0.3M KCL, 2mM DTT, 0.1 M MOPSO, pH 7, VAPOR DIFFUSION, HANGING DROP, temperature 277K |