2PRD
CRYSTAL STRUCTURE OF INORGANIC PYROPHOSPHATASE FROM THERMUS THERMOPHILUS
Experimental procedure
| Spacegroup name | H 3 2 |
| Unit cell lengths | 110.300, 110.300, 82.000 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 10.000 - 2.000 |
| R-factor | 0.153 |
| RMSD bond length | 0.015 |
| RMSD bond angle | 0.036 |
| Refinement software | PROLSQ |
Data quality characteristics
| Overall | |
| High resolution limit [Å] | 2.000 * |
| Number of reflections | 11673 |
| Completeness [%] | 90.0 * |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion * | 7.5 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | drop | protein | 15 (mg/ml) | |
| 2 | 1 | drop | Tris-HCl | 20 (mM) | |
| 3 | 1 | drop | ammonium sulfate | 47 (%) | |
| 4 | 1 | drop | MPD | 3 (%) | |
| 5 | 1 | drop | 2 (mM) |
