2POO
THERMOSTABLE PHYTASE IN FULLY CALCIUM LOADED STATE
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | MACSCIENCE M18X |
| Temperature [K] | 297 |
| Detector technology | IMAGE PLATE |
| Detector | MAC Science DIP-2020 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 50.980, 65.150, 105.680 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 8.000 - 2.050 |
| Rwork | 0.228 |
| R-free | 0.26200 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.500 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Refinement software | X-PLOR (3.8) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 20.000 |
| High resolution limit [Å] | 2.050 |
| Rmerge | 0.060 |
| Number of reflections | 21468 |
| Completeness [%] | 92.9 |
| Redundancy | 2.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | other * | 6.5 | This particular structure is not described in this paper. * |
