Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | NSLS BEAMLINE X4A |
| Synchrotron site | NSLS |
| Beamline | X4A |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2003-10-30 |
| Detector | ADSC QUANTUM 4 |
| Wavelength(s) | 1.0714 |
| Spacegroup name | P 64 |
| Unit cell lengths | 103.125, 103.125, 31.014 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 30.000 - 1.900 |
| R-factor | 0.195 |
| Rwork | 0.192 |
| R-free | 0.22620 |
| Structure solution method | SAD |
| RMSD bond length | 0.004 |
| RMSD bond angle | 1.280 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | CNS |
| Refinement software | CNS |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | 1.820 |
| High resolution limit [Å] | 1.760 | 1.760 |
| Number of reflections | 34549 | |
| <I/σ(I)> | 10.35 | 1 |
| Completeness [%] | 94.1 | 67.8 |
| Redundancy | 3.7 | 1.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6.9 | 298 | precipitant solution: NaSCN, Peg3350, pH 6.9, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
