2PAL

IONIC INTERACTIONS WITH PARVALBUMINS. CRYSTAL STRUCTURE DETERMINATION OF PIKE 4.10 PARVALBUMIN IN FOUR DIFFERENT IONIC ENVIRONMENTS

Experimental procedure

Spacegroup name	P 21 21 2
Unit cell lengths	59.560, 57.530, 26.270
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	7.000 * - 1.800
R-factor	0.172
RMSD bond length	0.018
RMSD bond angle	0.057
Refinement software	PROLSQ

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	9999.000 *
High resolution limit [Å]	1.800 *	1.800 *
Rmerge	0.073 *
Total number of observations	16690 *
Number of reflections	8816 *
Completeness [%]	80.0 *	74 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	sodium azide	3 (mM)