2P3F
Crystal structure of the factor Xa/NAP5 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Detector | RIGAKU RAXIS IV |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 137.170, 137.170, 167.670 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 8.000 - 3.100 |
R-factor | 0.18 |
Rwork | 0.180 |
R-free | 0.28000 |
Structure solution method | MOLECULAR REPLACEMENT |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | CNS |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 8.000 |
High resolution limit [Å] | 3.100 |
Number of reflections | 14108 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | 298 | Peg400, sodium citrate, pH 7.50, VAPOR DIFFUSION, HANGING DROP, temperature 298K |