2OV1

Crystal structure of apo form of ZnuA with flexible loop deletion

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	BRUKER AXS MICROSTAR
Temperature [K]	100
Detector technology	CCD
Collection date	2006-11-22
Detector	BRUKER SMART 6000
Wavelength(s)	1.5418
Spacegroup name	C 2 2 21
Unit cell lengths	62.578, 76.503, 127.151
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	50.000 - 2.500
R-factor	0.217
Rwork	0.217
R-free	0.24800
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1pq4
RMSD bond length	0.007
RMSD bond angle	1.308
Data reduction software	SAINT
Data scaling software	PROTEUM PLUS (PLUS)
Phasing software	MOLREP
Refinement software	CNS

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	2.550
High resolution limit [Å]	2.500	2.500
Number of reflections	10189
Completeness [%]	96.1	76.2
Redundancy	3	1.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1