2OTP
Crystal Structure of Immunoglobulin-Like Transcript 1 (ILT1/LIR7/LILRA2)
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2005-11-08 |
| Detector | RIGAKU RAXIS VII |
| Wavelength(s) | 1.5418 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 41.842, 72.971, 131.853 |
| Unit cell angles | 90.00, 90.32, 90.00 |
Refinement procedure
| Resolution | 30.000 - 2.600 |
| R-factor | 0.1765 |
| Rwork | 0.176 |
| R-free | 0.22710 |
| Structure solution method | AB INITIO |
| RMSD bond length | 0.011 |
| RMSD bond angle | 0.018 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | CNS |
| Refinement software | CNS |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 44.210 | 2.740 |
| High resolution limit [Å] | 2.500 | 2.500 |
| Rmerge | 0.074 | 0.320 |
| Number of reflections | 11930 | |
| <I/σ(I)> | 6.1 | 1.8 |
| Redundancy | 6.68 | 7.08 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 291.15 | 0.6M MgSO4, 0.1M Tris-Cl, pH 8.5, VAPOR DIFFUSION, HANGING DROP, temperature 291.15K |
