2ON7
Structure of NaGST-1
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RU200 |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2005-10-01 |
| Detector | RIGAKU RAXIS IV |
| Wavelength(s) | 1.5418 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 48.975, 80.683, 200.744 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 20.000 - 2.400 |
| R-factor | 0.19418 |
| Rwork | 0.190 |
| R-free | 0.28353 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | PDB 1TW9 |
| RMSD bond length | 0.017 |
| RMSD bond angle | 1.750 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | PHASES |
| Refinement software | REFMAC (5.2) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | 2.200 |
| High resolution limit [Å] | 2.100 | 2.100 |
| Rmerge | 0.073 | 0.344 |
| Number of reflections | 47226 | |
| <I/σ(I)> | 19.3 | 2.4 |
| Completeness [%] | 98.0 | 66.6 |
| Redundancy | 5.7 | 2.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 4.5 | 298 | PEG, acetate, pH 4.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
