2OKI
Crystal structure of dimeric form of PfFabZ in crystal form2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2003-09-01 |
Detector | MAR scanner 345 mm plate |
Wavelength(s) | 1.5418 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 71.966, 81.926, 91.629 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 23.280 - 2.700 |
R-factor | 0.258 |
Rwork | 0.258 |
R-free | 0.28600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1zhg |
RMSD bond length | 0.010 |
RMSD bond angle | 1.600 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.810 |
High resolution limit [Å] | 2.700 | 2.700 |
Rmerge | 0.056 | 0.290 |
Number of reflections | 8316 | |
<I/σ(I)> | 21.5 | 4.6 |
Completeness [%] | 96.4 | 90 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.5 | 300 | 30% PEG 4000, 0.1M acetate buffer pH4.5, 0.2M ammonium acetate, VAPOR DIFFUSION, HANGING DROP, temperature 300K |