2OHX

REFINED CRYSTAL STRUCTURE OF LIVER ALCOHOL DEHYDROGENASE-NADH COMPLEX AT 1.8 ANGSTROMS RESOLUTION

Experimental procedure

Spacegroup name	P 1
Unit cell lengths	51.760, 44.540, 94.610
Unit cell angles	104.80, 102.30, 70.60

Refinement procedure

Resolution	10.000 - 1.800
R-factor	0.173
Rwork	0.173
RMSD bond length	0.014
RMSD bond angle	2.910
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall
Low resolution limit [Å]	10.000 *
High resolution limit [Å]	1.800 *
Rmerge	0.080 *
Number of reflections	62440 *
Completeness [%]	88.5 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1	enzyme	1 (%)
2	1	2	TES	0.05 (M)
3	1	1	NADH		5mg
4	1	1	DMSO		0.5ml
5	1	2	NADH		5mg
6	1	2	DMSO		0.5ml