2OH5
The Crystal Structure of Infectious Cypovirus Polyhedra
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 120 |
| Detector technology | CCD |
| Collection date | 2006-08-05 |
| Detector | MAR CCD 165 mm |
| Wavelength(s) | 0.99830 |
| Spacegroup name | I 2 3 |
| Unit cell lengths | 102.777, 102.777, 102.777 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 18.760 - 1.980 |
| R-factor | 0.099 |
| Rwork | 0.093 |
| R-free | 0.15400 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.490 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Refinement software | REFMAC |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.000 | 2.050 |
| High resolution limit [Å] | 1.980 | 1.980 |
| Rmerge | 0.143 | 0.497 |
| Number of reflections | 12630 | |
| <I/σ(I)> | 13.9 | 4.3 |
| Completeness [%] | 99.0 | 100 |
| Redundancy | 7.3 | 7.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 298 | The microcrystals used to determine this structure were directly purified from cells, in vivo crystallization in the cytoplasm of the cell, temperature 298K |
