2OEX
Structure of ALIX/AIP1 V Domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X29A |
Synchrotron site | NSLS |
Beamline | X29A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-10-09 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.9792 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 63.861, 50.049, 130.171 |
Unit cell angles | 90.00, 101.13, 90.00 |
Refinement procedure
Resolution | 50.000 - 2.580 |
R-factor | 0.23122 |
Rwork | 0.228 |
R-free | 0.30249 |
Structure solution method | SAD |
RMSD bond length | 0.010 |
RMSD bond angle | 1.293 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SOLVE (2.10) |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.690 |
High resolution limit [Å] | 2.600 | 2.600 |
Rmerge | 0.078 | 0.204 |
Number of reflections | 23601 | |
<I/σ(I)> | 12.3 | 3.6 |
Completeness [%] | 92.4 | 64 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 277 | 14% PEG 3350, 0.16M magnesium formate, pH 8.0, VAPOR DIFFUSION, SITTING DROP, temperature 277K |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 277 | 14% PEG 3350, 0.16M magnesium formate, pH 8.0, VAPOR DIFFUSION, SITTING DROP, temperature 277K |